{"id":3624,"date":"2017-04-10T02:38:14","date_gmt":"2017-04-09T18:38:14","guid":{"rendered":"http:\/\/13.213.236.142\/www.merck-lifescience.com.tw\/?p=3624"},"modified":"2017-07-03T11:23:37","modified_gmt":"2017-07-03T03:23:37","slug":"purospher-star-hplc-columns-%e5%ad%b8%e5%90%8d%e8%97%a5%e6%aa%a2%e6%b8%ac%e7%94%a8%e9%80%99%e6%94%af%e5%b0%b1%e5%b0%8d%e4%ba%86","status":"publish","type":"post","link":"http:\/\/13.213.236.142\/www.merck-lifescience.com.tw\/purospher-star-hplc-columns-%e5%ad%b8%e5%90%8d%e8%97%a5%e6%aa%a2%e6%b8%ac%e7%94%a8%e9%80%99%e6%94%af%e5%b0%b1%e5%b0%8d%e4%ba%86\/","title":{"rendered":"Purospher STAR HPLC columns-\u5b78\u540d\u85e5\u6aa2\u6e2c"},"content":{"rendered":"<p>\u5728\u5404\u570b\u9678\u7e8c\u9032\u884c\u5065\u4fdd\u6539\u9769\u4e4b\u969b\uff0c\u5b78\u540d\u85e5\u5728\u85e5\u54c1\u5e02\u5834\u7684\u91cd\u8981\u6027\u65e5\u76ca\u91cd\u8981\uff0c\u800c\u5b78\u540d\u85e5\u7684\u5206\u6790\u4e5f\u662f\u88fd\u9020\u5546\u91cd\u8981\u7684\u8b70\u984c\u3002<br \/>\n\u5728\u5b78\u540d\u85e5\u6709\u6548\u6210\u5206\u53ca\u4e0d\u7d14\u7269\u7684\u5206\u6790\u7684\u65b9\u6cd5\u4e2d\uff0cHPLC\u7684\u65b9\u6cd5\u53c8\u70ba\u6700\u666e\u904d\u3002\u56e0\u6b64\u9ed8\u514b\u516c\u53f8\u91dd\u5c0d\u8fd1\u671f\u5c08\u5229\u5230\u671f\u7684\u6578\u7a2e\u5b78\u540d\u85e5\u958b\u767c\u51fa\u76f8\u5c0d\u61c9\u65bcUSP\u65b9\u6cd5\u7684\u5206\u6790\u65b9\u6cd5\u3002\u5176\u4e2d\u4e26\u4f7f\u7528\u4ee5\u9ad8\u7d14\u5ea6\u77fd\u81a0\u88fd\u9020\u7684Purospher STAR \u7ba1\u67f1\u4f5c\u70ba\u4e3b\u8981\u7684\u5206\u6790\u7ba1\u67f1\u3002Purospher STAR \u7ba1\u67f1\u9664\u4e86\u5176\u9ad8\u7d14\u5ea6\u77fd\u81a0\u9069\u65bc\u5206\u6790\u9178\u3001\u4e2d\u3001\u9e7c\u6027\u7269\u8cea\u5916\uff0c\u5176\u9178\u9e7c\u8010\u53d7\u7bc4\u570d\u4e5f\u8f03\u4e00\u822c\u77fd\u81a0\u7ba1\u67f1\u70ba\u5ee3(pH 1.5~10.5)\uff0c\u66f4\u5177\u6975\u4f73\u7684\u6279\u6b21\u6e96\u78ba\u5ea6\u8207\u7ba1\u67f1\u58fd\u547d\u3002\u56e0\u6b64\u9069\u7528\u65bc\u5927\u591a\u6578\u4e2d\u4f4e\u6975\u6027\u7269\u8cea\u7684\u5206\u6790\u3002<\/p>\n<p>\u672c\u6587\u8b39\u8209\u4e00\u500b\u4f8b\u5b50\u4f5c\u70ba\u5370\u8b49\u3002<br \/>\nUSP Method for Amlodipine Besylate Assay<br \/>\nPurospher STAR RP-18 endxapped<br \/>\nChromatographic Conditions<br \/>\nColumn: Purospher\u00aeSTAR RP-18 endcapped (5 \u03bcm) 125&#215;4.0 mm 1.50036.0001<br \/>\nInjection: 10 \u03bcL<br \/>\nDetection: Shimadzu Prominence, UV 237 nm<br \/>\nCell: 10 \u03bcL<br \/>\nFlow Rate: 1.0 mL\/min<br \/>\nMobile Phase<br \/>\n(v\/v):<br \/>\nBuffer: 7.0 ml triethyl amine in 800 ml of water. pH adjusted to 3.0 +\/<br \/>\nwith phoshoric acid. Dilute to 1 liter with water. Mix. Buffer, Methanol and<br \/>\nAcetonitrile 50:35:15(v\/v)<br \/>\nTemperature: Ambient<br \/>\nDiluent Mobile phase<br \/>\nSample: 40 ppm of Amlodipine in mobile phase<br \/>\nPressure Drop: 131 Bar (1900 psi)<\/p>\n<p><img loading=\"lazy\" class=\"alignnone size-full wp-image-1527\" src=\"http:\/\/13.213.236.142\/www.merck-lifescience.com.tw\/wp-content\/uploads\/2016\/10\/1450677590-2491979220.png\" alt=\"1450677590-2491979220\" width=\"562\" height=\"485\" srcset=\"http:\/\/13.213.236.142\/www.merck-lifescience.com.tw\/wp-content\/uploads\/2016\/10\/1450677590-2491979220-200x173.png 200w, http:\/\/13.213.236.142\/www.merck-lifescience.com.tw\/wp-content\/uploads\/2016\/10\/1450677590-2491979220-300x259.png 300w, http:\/\/13.213.236.142\/www.merck-lifescience.com.tw\/wp-content\/uploads\/2016\/10\/1450677590-2491979220-400x345.png 400w, http:\/\/13.213.236.142\/www.merck-lifescience.com.tw\/wp-content\/uploads\/2016\/10\/1450677590-2491979220.png 562w\" sizes=\"(max-width: 562px) 100vw, 562px\" \/><\/p>\n","protected":false},"excerpt":{"rendered":"<p> [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":3054,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":[],"categories":[121],"tags":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v18.8 - 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